Metrohm 850 Professional IC Anion MSM-HC MCS Prep 1 Instrukcja Użytkownika

850 Professional ICAnion MSM-HC – MCS – Prep 1 – 2.850.2120Manual8.850.8017EN

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VIII￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Figure 45 Removing valves ...

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭90￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1￭ Place the valve with the seal faced downwards

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭91123567891098710546Figure 47 Components of

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭92￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1￭ Place the valve housing over the stacked comp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭93Mounting the pump headNoteTo prevent the p

5.6 Inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭94￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Changing the filterThe flow must be stopped before c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭955.7 Inline sample preparationTo protect t

5.8 Rinsing the sample path￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭96￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1 2Aspirating the sample and measuring time

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭975.9 Sample degasser5.9.1 OperationIf you

5.11 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭98￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1The MSM-HC consi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭99 2Regenerating the MSM-HCCautionThe pump t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe instrument

5.11 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭100￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1123 45Figure 49

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭101￭ Check whether solution emerges at the M

5.11 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭102￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 15.11.3.3 Repla

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭103￭ Insert the new MSM-HC rotor A (49-3) in

5.12 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭104￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1CautionThe 6.1826.xxx pump tubings consist of P

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭105OrdernumberName Material InnerdiameterUse

5.13 Metrohm CO2 suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭106￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1 3Mounting filter screw￭ Screw the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭1075.14 Conductivity detector5.14.1 Mainte

5.15 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭108￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 15.15.2 ProtectionTo protect the separation co

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭1095.16 Quality Management and validation w

1.1 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1used for the purpose of protecting other sen

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭110￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 16 Troubleshooting6.1 Problems and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭111Problem Cause RemedyEluent – Evaporation of theorga

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭112￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Problem Cause RemedyMCS – vacuum pum

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭113Problem Cause Remedy￭ Replace separation column (se

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭114￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Problem Cause RemedyEluent – Gas bub

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭1157 Technical specifications7.1 Reference

7.5 Housing￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭116￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 17.5 HousingDimensionsWidth 365 mmHeight 642 mmDepth 380

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭117Pressure rangePump 0…50.0 MPa (0…500 bar)P

7.10 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭118￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 17.10 Column thermostatType Peltier technique

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭1197.13 Metrohm CO2 suppressor (MCS)Material

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭3interactions with the column. The Metrohm analytical col

7.15 Mains connection￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭120￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Cell tempera-ture20…50 °C in increments of 5 °C

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭1217.17 Safety specificationDesign / Test ￭

8.1 Declaration of Conformity￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭122￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 18 Conformity and warranty8.1 Declarat

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭123EN 61010-1 Safety requirements for electric

8.3 Warranty (guarantee)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭124￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Software developmentSoftware development occ

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭125Faults arising from circumstances that are

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭126￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 19 AccessoriesCautionSubject to change without

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭127Qty. Order no. Description2 6.1608.020 Glass bottle / 1

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭128￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Qty. Order no. Description1 6.1803.040 PTFE cap

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭129Qty. Order no. Description2 6.1816.020 Silicone tubing

1.3 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 11.3 About the documentationCautionPlease r

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭130￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Qty. Order no. Description1 6.2057.080 Adsorpti

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭131Qty. Order no. Description1 6.2621.030 Hexagon key 4 mm

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭132￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Qty. Order no. Description1 6.2626.000 Drain no

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭133Qty. Order no. Description1 6.2744.020 Luer/UNF couplin

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭134￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Qty. Order no. Description3 6.2744.070 Pressure

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭135Qty. Order no. Description1 6.2816.020 Syringe 10 mL wi

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭136￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Qty. Order no. Description1 6.2837.000 CO2 adso

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭1379.2 Optional accessories 2.850.2120 850 Professional

9.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭138￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Order no. DescriptionFrench, Chinese, Korean

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭139IndexNumbers/Symbols6.2821.090 aspiration filter ... 826.282

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭51.4 Safety instructions1.4.1 General notes on safetyWa

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭140￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Protection ... 31, 82Technical specifications

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭141Separation column ... 75Rinsing time ...

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Protection against electrostatic chargesWarning

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭7More details about the disposal of your old equipment ca

2.1 Front￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 12 Overview of the instrument2.1 Front9123546781011121314Fig

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭93Purge valveFor deaerating the high pressu

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 12.2 Rear12221219201017157654318119121381416Figure 2 Rear 850

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭113Mains switchFor switching the instrument

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1CautionWhen connecting an instrument to the MSB connector (2-

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭133 Installation3.1 About this chapterThe Installation

3.2 Initial installation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1 3Connecting the eluent path￭ Equip the 6.183

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭15￭ Connect the capillary labeled with H20 with a 6.2744.

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.3 Installation diagramThe following instal

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭171222458910121415161718193333111362122720Figure 3 Instal

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13PEEK pressure screw, short 6.2744.0704MSM-HC

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭19For a detailed description of the dialysis and the comp

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Professional ICAnion MSM-HC – MCS – P

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 168131411032452791112Figure 4 Installation dia

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭213Tubing olive 6.2744.034For connecting capillaries to t

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1698132452712101113Figure 5 Installation diagr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭233Tubing olive 6.2744.034For connecting capillaries to t

3.5 Capillary connections in the IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.5 Capillary connections

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭25PEEK capillaries (poly-etheretherketone)PEEK capillarie

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.6 Rear of the instrument3.6.1 Rollers a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭27Removing rollersProceed as follows to remove the roller

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1211Figure 8 Handle as MPak holder1Knurled s

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭293.6.2 Positioning and connecting the detectorDetector

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1NoteUp to two detectors can be positioned a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭31￭ Connect the detector cable to the detector connection

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1123Figure 10 Connection for the leak sensor

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭33245613798Figure 11 Drainage tubing1Drainage tubing conn

3.7 Capillary and cable feed-throughs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 17Drainage tubingSection of the 6

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭35212134Figure 12 Capillary feed-throughs on the doors1Lu

3.7 Capillary and cable feed-throughs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 11234567 88 76 59101112 1211109Fr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭373.8 Eluent3.8.1 Connecting eluent bottleThe eluent is

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 11 234Figure 14 Installing eluent bottle attachment1Eluent a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭39 4Installing tubing weighting and aspiration filter1 23

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument d

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1￭ Fasten the bottle attachment (16-2) on the eluent bottle

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭415Eluent6Aspiration filter 6.2821.0907Filter holderFrom

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13Tubing flareWith tubing nipple.4Clamping scre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭4310891234562722211212213Figure 20 Capillary connections

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1NoteThe eluent aspiration tubing is already in

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭453.10.2 Deaerating the high pressure pumpThe high press

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Deaerating the high pressure pumpThe instrumen

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭47 4Setting the flow rate￭ Start MagIC Net (if not yet st

3.12 Pulsation damper￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Installing the inline filterCautionObserve the f

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭49The pulsation damper protects the separation column fro

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.11 Inline filter ...

3.13 Sample degasser￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.13 Sample degasserThe sample degasser removes

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭51 4Guide the other end of the connection capillary out o

3.14 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13Connection capillaryConnected to connector 4. Ca

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭53124 53 6124 53 6124354312A BFigure 27 Injection valve –

3.15 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.15 Column thermostatThe column thermostat co

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭5513211112Figure 28 Column thermostat1Capillary feed-thro

3.15 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1NoteThe column input capillary is already threa

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭573.16 High Capacity Metrohm Suppressor Module(MSM-HC)3.

3.16 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 113234567821Figur

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭59Connecting the capillaries of the MSM-HC 1Connecting th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭V5.5 High pressure pump ...

3.17 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.17 Peristaltic pump3.17.1 Principle of the p

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭613.17.2 Installing the peristaltic pump6.2744.16016.274

3.17 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1 3Connecting the pressure sideNoteDepending on t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭63123Figure 33 Install pump tubing connection without fil

3.17 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Pump tubing Adapter6.1826.340 (black/black)6.182

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭653.18 Metrohm CO2 suppressor (MCS)3.18.1 General infor

3.18 Metrohm CO2 suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13Aspirating capillaryFor aspirating

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭67938 7312 33456Figure 35 Adsorption cartridge holder1PEE

3.19 Conductivity detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1 2Removing the caps￭ Remove the two locking

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭69213Figure 36 Conductivity detector front1IC detector 1.

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 17.7 High pressure pump ...

3.19 Conductivity detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1132Figure 37 Conductivity detector rear1Det

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭713 21Figure 38 Connection detector – MCS1Detector input

3.21 Guard column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1The mains cable is three-core and provided with a pl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭73NoteThe guard column may only be installed after the in

3.22 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 13.22 Separation columnThe intelligent separati

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭75Connecting and rinsing the separation column 1Connectin

4.1 Initial start-up￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 14 Start-upThe chapter Start-up is divided into 2

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Start-up850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭77 4Setting the contact pressure of the peristaltic pumpNoteT

4.2 Conditioning￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1 2Preparing the instrument￭ Ensure that the column is

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭795 Operation and maintenance5.1 General i

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭VIITable of figuresFigure 1 Front 850 Professional IC –

5.2 Capillary connections￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 15.1.3 OperationCautionIn order to avoid dis

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭815.3 DoorCautionThe door is made of PMMA (

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 15.4.2 Operation5.4.2.1 Supply bottleThe suppl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭83CautionIn order to spare the pump seals, t

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭84￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1Cleaning/replacing the zirconium oxide pistonCl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭85￭ Remove the backup ring from the pump hea

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭86￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 1parts: a tip for removing the old piston seal a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭8712Figure 42 Removing the piston seal1Pisto

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭88￭￭￭￭￭￭￭￭850 Professional IC – Anion MSM-HC – MCS – Prep 112Figure 44 Inserting the piston seal into the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC – Anion MSM-HC – MCS – Prep 1￭￭￭￭￭￭￭￭891234Figure 45 Removing valves1Outlet valve