Metrohm 797 VA Computrace Instrukcja Użytkownika Strona 170
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6 Electroplating Bath VA
797 VA Computrace – Software
158
Area
Peak area between peak curve and calculated
baseline.
Derivative
Difference between positive an negative maximum
of the first derivative of the voltammogram.
Coulometric
Charge transmitted during the peak.
Smooth factor [ 1...6 ; 4 ]
Smoothing power of the Savitzky/Golay smooth-
ing of the baseline (1 = minimum smoothing, 6 =
maximum smoothing) (see Smoothing and differ-
entiation, section 5.8).
Eliminate spikes
Eliminates spikes to smooth the signal.
Reverse sweep [ on, off ; off ]
Enable peak evaluation of the reverse sweep of
cyclic sweeps (not available with CPVS).
LAT Standard addition for brighteners
Linear Approximation Technique (“LAT Standard addition for
brighteners”) is a Calibration technique for CVS and CPVS. It is
mainly used to analyze Brighteners in electroplating baths. It is cho-
sen, if the difference between Q(“Intercept solution” + “Bath solu-
tion”) and Q(only “Intercept solution”) is too small to use “MLAT
Standard addition for brighteners”.
The "Intercept value" needed for the calculation can be recorded
and adopted automatically with the Calibration technique "LAT Re-
cord intercept value".
Note: If possible, “MLAT” should be the preferred
Calibration tech-
nique for Brightener determination. With “MLAT”, “Intercept solu-
tion” and “Bath solution” are measured successively in the same
method run, what minimizes fluctuations caused by solution ex-
change and time displacement of the measurements.
Note: A determined "Intercept value" is only adopted automati-
cally if the checkbox Save calibration curves additionally without
date and time
on the General tab of the GENERAL SETTINGS win-
dow is checked.
Determination tab with Calibration technique “LAT”
The Determination tab of the EDIT WORKING METHOD PARAME-
TERS
window contains general specifications for performing the
determination. The parameters displayed depend on the selected
Calibration technique and measurement Technique. With “LAT
- 797 VA Computrace 1
- Table of contents 10
- Table of contents 11
- 1 Introduction 13
- 1.2 General information 14
- 1.3 Installation 14
- 1.3 Installation 15
- 1 Introduction 16
- 1.5 Overview of file types 19
- 1.6 Context sensitive menus 20
- 2 Main window 21
- 2 Main window 22
- 2.3 File menu 24
- 2.3 File menu 25
- 2.4 Mode menu 27
- 2.5 Utility menu 28
- 2.6 User menu 28
- 2.6 User menu 29
- 2.7 Settings menu 32
- 2.7 Settings menu 33
- 2.8 Window menu 46
- 2.8 Window menu 47
- 3.1 Electrodes 48
- 3.1 Electrodes 49
- Drop size [ 1...9 ; 4 ] 50
- 3.2 VA measurement modes 52
- 3.2 VA measurement modes 53
- METHOD SPECIFICATIONS 54
- KING METHOD SPECIFICATIONS 56
- Normal pulse 58
- 3.3 Potentiostat 71
- 3.5 Graphical settings 76
- 3.5 Graphical settings 77
- Color of the line 81
- 4 Exploratory mode 82
- 4 Exploratory mode 84
- 4.3 Exploratory curves 86
- 4.3 Exploratory curves 87
- PLORATORY CURVES 97
- EXPLORA 97
- TORY SPECIFICATION 97
- 5 Determination mode 98
- 5 Determination mode 100
- 797 VA Computrace – Software 101
- 5.3 Monitor 120
- 5.3 Monitor 121
- 5.4 Determination curves 130
- 5.4 Determination curves 131
- 5.5 Results 141
- 5.5 Results 143
- Electrode test 145
- 5.6 Sample table 146
- 5.6 Sample table 147
- Voltammogram 154
- Chronoamperogram 154
- Minimum 157
- Recommended 157
- 6 Electroplating Bath VA 162
- Calibra 205
- Calibration 205
- Calibration tech 207
- 7 Manual control 209
- 7 Manual control 210
- 7.2 Dosing Device control 211
- 7.3 Pump control 212
- 7.4 Film deposition 213
- 7.5 Cleaning procedure 215
- 8 How to ...? 217
- 8.2 User rights 218
- DOSINOS window: 239
- Suppressor standard 247
- Rinsing solution 247
- Response curve) 253
- 8.10 Diagnostic procedures 265
- 9 Troubleshooting 269
- 9.4 Dosing Device problems 270
- 9 Troubleshooting 272
- AC – Alternating 273
- FICATION 273
- METHOD PARAMETERS 273
- 9.6 Voltammetric problems 274
- 9.6 Voltammetric problems 275
- Software license 288
- Software license 289
- Index 291
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