Metrohm IC Net 2.0 Instrukcja Użytkownika

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Strona 1 - IC Net 2.0

Metrohm Ltd.CH-9101 Herisau/SwitzerlandPhone ++41 71 353 85 85Fax ++41 71 353 89 01Internet www.metrohm.chE-Mail [email protected]

Strona 2 - All Rights Reserved

1 IntroductionIC Net 2.02Section 5 InterfacesInstallation, control and parameter settings of in-terfacesSection 6 DevicesInstallation, control and pa

Strona 3 - Table of contents

6 DevicesIC Net 2.092Ctrl "controlcommand"Set the specified remote outputsignal. In addition to the normalcontrol commands (details see 766

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6.11 766 IC Sample ProcessorIC Net 2.093Beaker positionsRack type Current rack type (read-only).Parameter Name for special beaker position.Pattern Nu

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6 DevicesIC Net 2.094ControlParameter Name for special control command.Pattern Remote line settings for special controlcommand.<Add> Add a new

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6.11 766 IC Sample ProcessorIC Net 2.095ScanParameter Name for special scan command.Pattern Remote line settings for special scancommand.<Add>

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6 DevicesIC Net 2.0966.12 Data recorder6.12.1 Data recorder iconThe Data recorder icon is one of the components always pres-ent in a new SYSTEM win

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6.12 Data recorderIC Net 2.097Processing method Name of the method file (*.mtw) linked tothe system.<show> Open processing method.<choose>

Strona 9 - 1 Introduction

6 DevicesIC Net 2.0986.13 System timer6.13.1 Timer iconThe system timer is used for programming system tasks whichare started automatically daily o

Strona 10 - 1.3 Notation and pictograms

7.1 Method file handlingIC Net 2.0997 MethodsA method contains all information necessary for data acquisi-tion, integration, peak evaluation and qua

Strona 11 - 1.4 Installation

7 MethodsIC Net 2.01007.2.1 GeneralTab General of the passport with general description of themethod and determination.Ident User defined identifier

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7.2 PassportIC Net 2.0101Run Number of the current run starting from thevery first one. All runs are automaticallynumbered by the system (read-only).

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1.4 InstallationIC Net 2.03<OK>Button[ Ctrl ] KeyHazardThis symbol draws attention to a possibledanger to life or of injury if the associateddi

Strona 14 - 2.2 Glossary

7 MethodsIC Net 2.0102Internal standard amountConcentration of the internal standardcomponent for relative concentration cal-culations.Date/time when

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7.2 PassportIC Net 2.01037.2.4 EluentTab Eluent of passport with eluent information.Eluent A Description of eluent composition (max.256 characters).

Strona 16 - 2.4 Main window elements

7 MethodsIC Net 2.01047.2.5 CommentTab Comment of passport for entry of free-text user commentsinto the chromatogram description. Use this feature t

Strona 17 - 2.5 Icons of the main window

7.2 PassportIC Net 2.0105<Add new> Add a new GLP comment to the MethodLog. Text can be entered in the New com-ment window, date/time and logged

Strona 18 - 2.6 Overview of file types

7 MethodsIC Net 2.01067.3 Method setupIC NET / Method / Method setupThis menu item opens the Method setup window which includesthe most common param

Strona 19 - 2.7 Context-sensitive menus

7.3 Method setupIC Net 2.01077.3.3 FiltersTab Filters of Method setup window with parameters for noise fil-tration of raw data. Three different filt

Strona 20 - 2.9 Help

7 MethodsIC Net 2.01087.3.4 ProcessingTab Processing of Method setup window for definition of actionsthat are performed during the run or when the c

Strona 21 - 3 Software settings

7.3 Method setupIC Net 2.0109Program before Name and path of the program to bestarted automatically before the run isstarted.Program after Name and p

Strona 22 - 3.3 Global settings

7 MethodsIC Net 2.0110European PharmacopoeiaFormula setting according to EuropeanPharmacopoeia.US Pharmacopoeia Formula setting according to US Pharm

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7.4 IntegrationIC Net 2.01117.4 Integration7.4.1 General informationIC NET / Method / IntegrationThis menu item opens the Integration parameters wi

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1 IntroductionIC Net 2.04The two software packages «IC Net 2.0» and «Autodatabase1.0» will be installed in the desired directory. Icons are created i

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7 MethodsIC Net 2.01127.4.2 SetupTab Setup of Integration parameters window with integration pa-rameters. The two most important of these parameters

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7.4 IntegrationIC Net 2.0113width of the narrowest peak on the chro-matogram (normally 2…10 s).Entry range: 0.1……480 sBroadening Broadening for peak

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7 MethodsIC Net 2.0114<Suggest> This function sets up reasonable integrationparameters in the following way:• Slope is set to a reasonable val

Strona 28 - 4.3 System functions

7.4 IntegrationIC Net 2.0115If an integration event is added or modified, the Edit integrationevent window is opened where the following parameters c

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7 MethodsIC Net 2.0116Integration events for peak start/endSet peak start Force the beginning of a new peak. If apeak is available at the moment of t

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7.4 IntegrationIC Net 2.0117Set horizontal baseline Set horizontal baseline for all peaks exceptthe last one of adjacent peaks that are notseparated.

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7 MethodsIC Net 2.0118Force horizontal Cancel horizontalbase back base backForce horizontal base backSet horizontal baseline for a single peak.The ba

Strona 32 - 4.4 System settings

7.5 Calibration and quantificationIC Net 2.01197.5 Calibration and quantification7.5.1 General informationThe aim of any chromatographic analysis i

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7 MethodsIC Net 2.01207.5.2 NotationsR Stands for response value, either area or height,depending on setting selected in the Calibrationgraphs windo

Strona 34 - 4.5 System state window

7.5 Calibration and quantificationIC Net 2.01217.5.3 External standard calibrationExternal standard calibration (absolute calibration) is a key way

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2.1 Starting/closing the programIC Net 2.052 Fundamentals of the operation2.1 Starting/closing the program2.1.1 Start the «IC Net» programStart th

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7 MethodsIC Net 2.0122Number Row number (read-only).Peak Number of the peak in the chromatogramthat corresponds to the given component.If this field

Strona 37 - 5 Interfaces

7.5 Calibration and quantificationIC Net 2.0123min C (max C) Minimum (Maximum) concentrationvalue for the component. Componentswhose concentration le

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7 MethodsIC Net 2.01247.5.5 Peak identificationIC NET / Method / Calibration / IdentificationSelecting this menu item or clicking on <Identificat

Strona 39 - 5.2 762 IC Interface

7.5 Calibration and quantificationIC Net 2.0125Worst case... Information on the component with theworst (largest) deviation of actual and ex-pected r

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7 MethodsIC Net 2.0126Level 1...Level N Contains concentrations (or other chosenvalues) of components for correspondingCalibration level.<Add>

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7.5 Calibration and quantificationIC Net 2.01277.5.7 Calibration curveIC NET / Method / Calibration / GraphsSelecting this menu item or clicking on

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7 MethodsIC Net 2.0128Calibration points tableThis table contains the basic information used to construct thecalibration curve:Level Number of Calib

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7.5 Calibration and quantificationIC Net 2.0129Base Base for calculations (Area or Height) inquantification and calibration procedures.Indicates, wh

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7 MethodsIC Net 2.0130Coef. (balance) Recalculate coefficient of the universal com-ponent. The aim of this action is to adjust theresponse factor of

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7.6 Report outputIC Net 2.01317.6 Report output7.6.1 Report options windowIC NET / Method / Report optionsIC NET / Process / Make reportThe Report

Strona 46 - 5.3 771 Compact Interface

2 Fundamentals of the operationIC Net 2.062.2 GlossaryBatch reprocessingBatch reprocessing is understood to be the subsequent reproc-essing of a ser

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7 MethodsIC Net 2.01327.6.2 Items to reportThis part of the Report options window contains a list of importantreport items that can be included into

Strona 48 - 5.4 761 Compact IC

7.6 Report outputIC Net 2.0133Chromatogram plot Plot of the chromatogram (only for Printer orFile destination).Peak table Peak table with results.

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7 MethodsIC Net 2.0134DATA GLP LOGAnalysing data of channel :ch1Time constant, ms: 100.00; old 100.01Iterations: 2; Outliers: 1Sigma: 0.0Rejection di

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7.6 Report outputIC Net 2.0135Calibration defaults Calibration parameters defined in the com-ponent window and on the Math tab of theMethod setup win

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7 MethodsIC Net 2.0136Channel table Parameters of the data acquisition channelused. CHANNELS TABLEch1 No Name Units Input Minimum Z

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7.6 Report outputIC Net 2.01377.6.4 Report destinationThe following output devices can be selected simultaneously inany combination as targets for r

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7 MethodsIC Net 2.0138As long as no universal component is de-fined, only peaks with non-zero concentra-tions are listed.The peak table includes the

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7.6 Report outputIC Net 2.0139Concentration of std Concentration of the internal standardcomponent for relative concentration cal-culations. This val

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7 MethodsIC Net 2.01407.6.6 Template optionsFor report output using a report template the following parame-ters can be modified:Template Selection o

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7.6 Report outputIC Net 2.01417.6.8 Report elementsIf Quantification method = Custom has been selected, the peak ta-ble can be customized on the use

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2.2 GlossaryIC Net 2.07baselines. The integration algorithm included in the program isinfluenced by the integration parameters and the optionallyprog

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7 MethodsIC Net 2.0142effectivity, TP Effectivity for the peak in number of theo-retical plates. The number of theoreticalplates Ni per column for a

Strona 59 - 5.6 Global timer

7.6 Report outputIC Net 2.0143Total value for the column is the sum ofconcentrations for all components.concentration% Normalization of concentration

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7 MethodsIC Net 2.0144type The types of components are designatedby a one-letter code:R Reference component (used for peak iden-tification).S Stand

Strona 61 - 6 Devices

8.1 Chromatogram windowIC Net 2.01458 Chromatograms8.1 Chromatogram windowThe CHROMATOGRAM window is used to show a running or re-corded chromatogr

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8 ChromatogramsIC Net 2.0146During active data acquisition the elapsed time, the duration ofthe chromatogram or program and the current X and Y value

Strona 63 - 6.2 Watch window

8.2 Chromatogram file handlingIC Net 2.0147Filename Filename (common wildcards as * and ?are possible).Selected Number of selected chromatograms andt

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8 ChromatogramsIC Net 2.01488.2.2 Save chromatogramIC NET / File / Save / ChromatogramSave the selected chromatogram in a chromatogram file (*.chw)i

Strona 65 - 6.3 732 IC Detector

8.2 Chromatogram file handlingIC Net 2.0149Represent raw data as Output of raw data:Default units (float) Y values are exported in default units for

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8 ChromatogramsIC Net 2.01508.3 Graphical representation8.3.1 AppearanceIC NET / View / AppearanceThis menu item opens the Appearance window. It de

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8.3 Graphical representationIC Net 2.0151Response axisY from Beginning of the window on Y axis.Y to End of the window on Y axis.Tic marks Plot axes

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2 Fundamentals of the operationIC Net 2.082.3 Overview of program windows«IC Net 2.0» consists of different windows whose functionality islinked tog

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8 ChromatogramsIC Net 2.0152Component name Name of the component.Component name + QuantityName and quantity of the component.Channel labels Label fo

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8.3 Graphical representationIC Net 2.0153ColorsTab Colors of the Appearance window with color settings parame-ters for chromatograms.this color is de

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8 ChromatogramsIC Net 2.01548.3.2 Other graphical functionsIC NET / View / X full scaleBy selecting this menu item or pressing [ Ctrl ] + [ Home ] t

Strona 72 - 6.4 733 IC Separation Center

8.4 Peak editorIC Net 2.01558.4 Peak editor8.4.1 Switching on/off the peak editorIC NET / Process / Peak editorThe peak editor mode is used for sub

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8 ChromatogramsIC Net 2.0156IC NET / Peak / Select end pointMove the cursor to the end of the nearest peak and select thepeak.IC NET / Peak / Select

Strona 74 - 6.5 709 IC Pump

8.5 PrintingIC Net 2.01578.5 Printing8.5.1 Page layout for printingIC NET / File / Page layoutThe selection of this menu item or clicking on <Pa

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8 ChromatogramsIC Net 2.01588.5.2 Printer settingsIC NET / File / Printer setupBy selecting this menu item the Print setup window is openedwhere pri

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8.6 Miscellaneous functionsIC Net 2.01598.6 Miscellaneous functions8.6.1 ReintegrationIC NET / Process / ReintegrateThis menu item opens the Integr

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8 ChromatogramsIC Net 2.01608.6.4 Data compressionIC NET / Process / More / CompressSelection of this menu item opens the Raw data compression win-d

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8.6 Miscellaneous functionsIC Net 2.01618.6.6 AutodatabaseIC NET / Method / AutodatabaseThe Autodatabase options window contains parameters and set-

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2.5 Icons of the main windowIC Net 2.092.5 Icons of the main windowThe following icons are displayed in the IC NET main window:Open chromatogramSave

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8 ChromatogramsIC Net 2.0162

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9.1 Sample queue file handlingIC Net 2.01639 Sample queueA sample queue is a table containing sample-specific datawhich is used to facilitate work w

Strona 82 - 6.7 752 Pump Unit

9 Sample queueIC Net 2.01649.2 Sample queue control9.2.1 Sample queue overview tableIC NET / File / Open / Sample queueSYSTEM / System / Sample que

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9.2 Sample queue controlIC Net 2.0165Amount Sample amount. If this value is different forthe calibration run (c) and the sample run(s), the component

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9 Sample queueIC Net 2.01669.2.4 Cancel last runSAMPLE QUEUE OVERVIEW / Control / Cancel last runCancel the last run (set Started = 0 for this row).

Strona 85 - 6.8 753 Suppressor Module

9.3 Sample queue editorIC Net 2.0167Vial Autosampler vial position to take samplefrom.Volume Injected volume of sample in µL.Dilution Sample dilution

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9 Sample queueIC Net 2.0168QUEUE EDITOR / Edit / Paste row(s)Paste the rows from the clipboard into the sample queue table.QUEUE EDITOR / Edit / Dele

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10.1 Batch reprocessing queue file handlingIC Net 2.016910 Batch reprocessingReprocessing is understood to be the subsequent reprocessingof a series

Strona 88 - 6.9 754 Dialysis Unit

10 Batch reprocessingIC Net 2.017010.1.3 Save batch reprocessing queueQUEUE EDITOR / File / SaveSave the batch reprocessing queue in a batch reproce

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10.2 Perform batch reprocessingIC Net 2.0171Use method from file for reprocessingSelection of the desired chromatogram filewhose method should be use

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2 Fundamentals of the operationIC Net 2.0102.6 Overview of file typesThe following file types are produced by the «IC Net» software:*.adb Autodataba

Strona 91 - 6.10 750 Autosampler

10 Batch reprocessingIC Net 2.0172bration parameters (component table, con-centration table and calibration curve) areapplied to all sample runs.Appl

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10.2 Perform batch reprocessingIC Net 2.0173Modify chromatogram appearanceIf this option is enabled, the chromatogramAppearance parameters which have

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10 Batch reprocessingIC Net 2.017410.2.2 Merge chromatogramsREPROCESS / <Merge>Combine all chromatograms of the batch reprocessing queueinto a

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10.3 Batch reprocessing queue editorIC Net 2.017510.3 Batch reprocessing queue editor10.3.1 Open batch reprocessing queue editor windowREPROCESS /

Strona 95 - 6.11 766 IC Sample Processor

10 Batch reprocessingIC Net 2.0176Sample Info 1 First sample description. Will be placed intoappropriate passport field.Sample Info 2 Second sample d

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11.1 Software licenseIC Net 2.017711 Appendix11.1 Software licenseAs the purchaser of the «IC Net 2.0» PC software you also receivethe license to u

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11 AppendixIC Net 2.017811.3 Index%%B ...71,72%C ...

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11.3 IndexIC Net 2.0179ADC response...149Add level...

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11 AppendixIC Net 2.0180Calibration graph size ...157Calibration level...23,100,125,1

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11.3 IndexIC Net 2.0181Control lines...89Copy concentrations from level...

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2.7 Context-sensitive menusIC Net 2.011*.rtt Report file (ASCII file)Contains a report template.The *.rtt file is stored in the program folder.*.smt

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11 AppendixIC Net 2.0182Eluent B...103Eluent C...

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11.3 IndexIC Net 2.0183IIC Applications Collection (8.732.2013)...2IC pump ...

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11 AppendixIC Net 2.0184MMain windowelements...8icons...

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11.3 IndexIC Net 2.0185PPacking material ...102Page layout ...

Strona 106 - 6.13 System timer

11 AppendixIC Net 2.0186RRack definitions...92Rack type...

Strona 107 - 7 Methods

11.3 IndexIC Net 2.0187Save chromatogram after the run...108<Save defaults> ...

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11 AppendixIC Net 2.0188program...98TTab size...

Strona 109 - • Amount

All Rights Reserved.Printed in Switzerland by Metrohm AG, CH-9101 Herisau 2000

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2 Fundamentals of the operationIC Net 2.012[ PageDown ] Shifts a chromatogram on 1/10 part of ascreen downwards.[ Shift ] + [ up ] Increases a distan

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3.1 FontsIC Net 2.0133 Software settings3.1 FontsIC NET / Options / FontsThis option allows the selection of fonts used by the system.Font for dial

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3 Software settingsIC Net 2.014ences, open the Workplace window, changehardware settings of interfaces and devices,and change Security options.Admini

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3.3 Global settingsIC Net 2.015Data file overwrite Global settings for overwriting of chroma-togram files:Never Chromatogram files cannot be overwrit

Strona 114 - 7.3 Method setup

3 Software settingsIC Net 2.016Ignore last data directoryIf this option is enabled, the directory isopened where the current selected chro-matogram i

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4.1 System creationIC Net 2.0174 SystemsThe combination of Metrohm and Bischoff devices connected toan interface is called a system. The system incl

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4 SystemsIC Net 2.018<Add to workplace>, the interface icon will appear on the toolbar(PC Boards will not appear on toolbar).After clicking on

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4.1 System creationIC Net 2.019After clicking on <Finish>, the user is asked to save the new sys-tem as a system filesystem file (*.smt) in the

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4 SystemsIC Net 2.0204.2 System file handlingThe following menu items are used for opening, changing, savingand closing of systems:IC NET / File / O

Strona 119 - 7.4 Integration

4.3 System functionsIC Net 2.021SYSTEM / Control / Disconnect from workplaceDisconnect selected system from the workplace. If a system isdisconnected

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Table of contentsIC Net 2.0ITable of contents1 Introduction...1

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4 SystemsIC Net 2.0224.3.3 Start/stop determinationsSYSTEM / Control / Start determinationStart determination using the settings of the selected sys

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4.3 System functionsIC Net 2.023Ident User defined identifier (title) for the chro-matogram to be displayed in the title bar ofthe chromatogram windo

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4 SystemsIC Net 2.0244.4 System settings4.4.1 Modify system windowSYSTEM / Setup / Drag iconsIf this option is enabled, the device icons can be res

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4.4 System settingsIC Net 2.025Start with inject The time program of the loaded object orthe data acquisition (RECORDER) is startedat the moment the

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4 SystemsIC Net 2.0264.4.7 Show system parametersSYSTEM / Setup / Parameters / Startup hardwareDisplay of the name of the method linked to the syste

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4.5 System state windowIC Net 2.027RunningRunning program or chromatogram dataacquisition.Running program(xxx min left)Running time program with time

Strona 127 - Component table

4 SystemsIC Net 2.028E295Storage of memory values failed (repeatlast action; if error reappears, call Metrohmservice).E296Instrument stopped (restart

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5.1 Interface installationIC Net 2.0295 InterfacesThe «IC Net» program supports remote control for interfacesavailable from Metrohm and Bischoff. In

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5 InterfacesIC Net 2.030Details to the other steps of the system wizard procedure (in-stallation of devices, processing method, and data source) sees

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5.2 762 IC InterfaceIC Net 2.0315.2 762 IC Interface5.2.1 762 IC Interface featuresThe Metrohm 762 IC Interface is available as a one system ver-si

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Table of contentsIC Net 2.0II4.3 System functions...204.3.1 Connect and disconnec

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5 InterfacesIC Net 2.0325.2.4 762 IC Interface window762 icon / OpenThe 762 IC Interface window for parameter settings is opened byselecting this me

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5.2 762 IC InterfaceIC Net 2.033<ASK> Read current parameters from 762 IC In-terface.<SET> Send current parameters to 762 IC Inter-face.R

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5 InterfacesIC Net 2.034LinksThe Links tab of the 762 IC Interface is used for COM port selectionand settings.Alias Name of the interface or device.C

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5.2 762 IC InterfaceIC Net 2.035Time programOn the Program tab of the 762 System [#] window a user-definedtime program for the event output lines of

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5 InterfacesIC Net 2.036<Add> Add new program instruction.<Delete> Delete selected program instruction.<Verify> Test the time progr

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5.2 762 IC InterfaceIC Net 2.037Event command (2nd column)Setting the event output lines 1…7.Selection:0 (line off, inactive, open)1 (line on, active

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5 InterfacesIC Net 2.0385.3 771 Compact Interface5.3.1 771 Compact Interface featuresThe Metrohm 771 Compact Interface is a two channel Analog-to-D

Strona 139 - 7.6 Report output

5.3 771 Compact InterfaceIC Net 2.039Range Range for AD converter.Example: converts ± 2500 mV to 224 bitsEntry range: 2500, 1250, 625, 312.5, 156.25,

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5 InterfacesIC Net 2.040Handshake Enable/disable software handshake mode.Selection: Swchar, noneDefault value: SWchar<ASK> Read current paramet

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5.4 761 Compact ICIC Net 2.0415.4.3 761 icon in the system windowSystem disconnected System connected System connectedInjection valve in Injection

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Table of contentsIC Net 2.0III6 Devices ...536.1 Device

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5 InterfacesIC Net 2.042Conductivity, µµS/cm Live display of measured conductivity.Pressure, MPa Live display of measured pressure.The color settings

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5.4 761 Compact ICIC Net 2.043IC pump High-pressure pump.<On> Start high-pressure pump.<Off> Stop high-pressure pump.Peristaltic pump Per

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5 InterfacesIC Net 2.044Pressure max, MPa Startup value for maximum pressure limitfor high-pressure pump.Entry range: 0.0 ... 25.0 MPaPressure min, M

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5.4 761 Compact ICIC Net 2.045Second column Program instruction (see below).In addition to these predefined instructions,user-defined remote commands

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5 InterfacesIC Net 2.046Program END, RESET The END flag can be used to end aprogram, especially if the programtime should be longer than thechromatog

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5.4 761 Compact ICIC Net 2.047ConfigurationThe Configuration tab in the system settings window containsconfiguration settings for the 761 Compact IC.

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5 InterfacesIC Net 2.0485.4.5 Hardware settingsSelection of the Hardware menu item of the 761 icon using the rightmouse button opens the hardware se

Strona 150 - • L / (N

5.4 761 Compact ICIC Net 2.049Cell constant Cell constant of the conductivity cell forcorrect display of the absolute conductivity.Enter the cell con

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5 InterfacesIC Net 2.050Hardware error Hardware error detected at the 761 Com-pact IC (high-pressure pump, injectionvalve, or suppressor not working

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5.5 Metrohm PC BoardIC Net 2.0515.5 Metrohm PC BoardThe 2.714.0310 Metrohm PC Board Interface is a two channelAnalog-to-Digital Converter (often abb

Strona 153 - 8 Chromatograms

Table of contentsIC Net 2.0IV6.12 Data recorder ...966.12.1 Data recorder i

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5 InterfacesIC Net 2.0525.6.2 Timer programThe Timer window contains the user-defined program for sys-tem tasks. These tasks are started automatical

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6.1 Device installationIC Net 2.0536 DevicesThe «IC Net» program supports remote control for Metrohm andBischoff instruments. Each instrument within

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6 DevicesIC Net 2.054For every device to be controlled with «IC Net», open the groupwhich contains this device, select the device and the Serial port

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6.2 Watch windowIC Net 2.0556.2 Watch window6.2.1 Watch window iconThe watch window icon is one of the components always pres-ent in a new SYSTEM w

Strona 158 - 8.3 Graphical representation

6 DevicesIC Net 2.056The colors of the watch window fields and of the SYSTEM STATEwindow can be changed by clicking the fields with the rightmouse bu

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6.3 732 IC DetectorIC Net 2.0576.3 732 IC Detector6.3.1 732 IC Detector featuresThe Metrohm 732 IC Detector is a conductivity detector for ionchrom

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6 DevicesIC Net 2.0586.3.3 732 IC Detector window732 icon / OpenThe 732 IC Detector window for parameter settings is opened byselecting this menu op

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6.3 732 IC DetectorIC Net 2.059Range Display of measuring range in µS/cm.Full scale Display of full scale range in µS/cm.Cell const. Display of cell

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6 DevicesIC Net 2.060Range Measuring range in µS/cmSelection: 100, 200, 500 µµS/cm and1, 2, 5, 10 mS/cmFull scale The full scale range (operating ran

Strona 163 - 8.4 Peak editor

6.3 732 IC DetectorIC Net 2.061The Program tab contains the two following subpages:Program Main time program with all programsteps.Remote configurati

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Table of contentsIC Net 2.0V8 Chromatograms ...1458.1 Chromatogram window ...

Strona 165 - 8.5 Printing

6 DevicesIC Net 2.062List of program instructionsThe following program instructions can be added to the time pro-gram on the Program subpage:Instruct

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6.3 732 IC DetectorIC Net 2.063Pmax 0.0 ... 25.0 MPa Set maximum pressure limit forthe high-pressure pump con-nected to the 732 IC Detector tothe des

Strona 167 - 8.6 Miscellaneous functions

6 DevicesIC Net 2.0646.4 733 IC Separation Center6.4.1 733 IC Separation Center featuresThe Metrohm 733 IC Separation Center is a thermally andelec

Strona 168 - Raw data compression win

6.4 733 IC Separation CenterIC Net 2.065If the system is connected and the 733 icon is clicked with theright mouse button, the following menu appears

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6 DevicesIC Net 2.066Suppressorin position Display of current suppressor status.<STEP> Switch suppressor module to next position.Auto Stepfill,

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6.5 709 IC PumpIC Net 2.0676.5.2 709 IC Pump iconThe 709 icon is available in the SYSTEM window if an Isocraticpump 709 or an Isocratic pump 709 for

Strona 171 - 9 Sample queue

6 DevicesIC Net 2.068Pressure Live display of current pressure in MPa.This field is also available for the WATCHWINDOW.Flow Live display of current f

Strona 172 - 9.2 Sample queue control

6.6 Metrohm solvent delivery unitIC Net 2.069AdvancedThe Advanced tab of the 709 IC Pump window is only available for aconnected system.Correction fa

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6 DevicesIC Net 2.0706.6.2 Metrohm SDU iconThe SDU icon is available in the SYSTEM window if an SDU(Solvent Delivery Unit) has been installed with t

Strona 174 - 9.3 Sample queue editor

6.6 Metrohm solvent delivery unitIC Net 2.071Pressure Live display of current pressure in MPa.This field is also available for the WATCHWINDOW.Flow L

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Table of contentsIC Net 2.0VI10 Batch reprocessing ...16910.1 Batch reprocessing queue

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6 DevicesIC Net 2.072ProgramThe Program tab of the SDU window contains a time program forthe pump control system to define eluent gradients.Flow Over

Strona 177 - 10 Batch reprocessing

6.6 Metrohm solvent delivery unitIC Net 2.073%D Individual flow rate for pump D in percent oftotal flow.Entry range: 0 ... 100 %Enabled Enable time p

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6 DevicesIC Net 2.0746.7 752 Pump Unit6.7.1 752 Pump Unit featuresThe Metrohm 752 Pump Unit is a 2-channel peristaltic pumpwhich is normally used f

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6.7 752 Pump UnitIC Net 2.075ManualThe Manual tab of the 752 Pump Unit window for manual operationis only available for a connected system.Pump<On

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6 DevicesIC Net 2.076Second column Program instruction (see below).Third column Parameter for program instruction (seebelow).ENABLED Enable program s

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6.8 753 Suppressor ModuleIC Net 2.0776.8 753 Suppressor Module6.8.1 753 Suppressor Module featuresThe Metrohm 753 Suppressor Module consists of a c

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6 DevicesIC Net 2.078ManualThe Manual tab of the 753 Suppressor Module window for manualoperation is only available for a connected system.Pump<On

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6.8 753 Suppressor ModuleIC Net 2.079First column Time at which program instruction is ap-plied.Entry range: 0.0 ... 999.9 minIf no time is entered,

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6 DevicesIC Net 2.0806.9 754 Dialysis Unit6.9.1 754 Dialysis Unit featuresThe Metrohm 754 Dialysis Unit is a unit for on-line sample di-alysis befo

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6.9 754 Dialysis UnitIC Net 2.081ManualThe Manual tab of the 754 Dialysis Unit window for manual opera-tion is only available for a connected system.

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1.1 Purpose of programIC Net 2.011 Introduction1.1 Purpose of program«ICNet 2.0» is the name of the data acquisition and control soft-ware for PC-c

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6 DevicesIC Net 2.082Second column Program instruction (see below).Third column Parameter for program instruction (seebelow).ENABLED Enable program s

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6.10 750 AutosamplerIC Net 2.0836.10 750 Autosampler6.10.1 750 Autosampler featuresThe Metrohm 750 Autosampler is a sampler for automatic sam-ple i

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6 DevicesIC Net 2.0846.10.3 750 Autosampler window750 icon / OpenThe 750 Autosampler window for parameter settings is opened byselecting this menu o

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6.10 750 AutosamplerIC Net 2.085Loop size is Size of the sample loop at the 733 ICSeparation Center. If the loop size is> 20 µL, only 3 injections

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6 DevicesIC Net 2.086Manual injectionSample vial numberNumber of sample vial to be used for man-ual injection.<Select> Selection of the vial nu

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6.11 766 IC Sample ProcessorIC Net 2.0876.11 766 IC Sample Processor6.11.1 766 IC Sample Processor featuresThe Metrohm 766 IC Sample Processor is a

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6 DevicesIC Net 2.088If the system is connected and the 766 icon is clicked with theright mouse button, the following menu appears:Open Open the 766

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6.11 766 IC Sample ProcessorIC Net 2.089Position Selection of the vessel to be placed at theneedle.Selection: sample, sample+1, spec.#, 1...nLift<

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6 DevicesIC Net 2.090Status displayThe current status of the 766 IC Sample Processor can be dis-played on the Current state subtab of the Manual tab

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6.11 766 IC Sample ProcessorIC Net 2.091Num Row number (read-only).Task Program instruction (see below).Parameter Parameter for program instruction (

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